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NECO GCE June/July 2023 FREE CHEMISTRY PRACTICALย QUESTION AND ANSWER ROOMย
(1a)
[TABULATE]
Burette Reading (cmยณ) | Rough | Titration I | Titration II
Final Reading (cmยณ) | 21.50 | 43.00 | 22.00
Initial Reading (cmยณ) | 0.00 | 21.50 | 00.00
Volume of A used (cmยณ) | 21.50 | 21.50 | 22.00
(1ai)
Average Volume of acid used = 21.50 + 21.50/2 = 21.50cmยณ
(1aii)
Solution B[Sodium trioxocarbonate (iv)] feels soapy
(1bi)
Conc. B in mol/dmยณ =?
Ca= 0.04, Va= 21.50cmยณ, na= 1
Cb= ? , Vb= 25.00cmยณ nb= 1
CaVa/CbVb = na/nb = 0.04ร21.50/Cbร25.00 = 1/1
Cb= 0.04ร21.50/25.00 = 0.86/25.00
Cb= 0.0344mol/dmยณ
(1bii)
Conc. of B in g/dmยณ = Conc. of B in mol/dmยณ ร molar mass of B
Molar mass of B(NaCOโ)= (23ร2) + 12 + (16ร3) = 106
:. Conc. of B in g/dmยณ = 0.0344ร106 = 3.6g/dmยณ
(1biii)
1 mole of NaโCoโ = 1mole of NaโSoโ
:. 0.0344 mole of NaโCoโ = 0.0344 mole of NaโSoโ
โ of mole= mass/ molar mass
Molar mass of NaโSoโ= (23ร2)+32+(16ร4)=142
:. 0.0344 = mass/142
Mass=142ร0.0344=4.9g
(1biv)
1 mole of NaโCoโ= 1 mole of COโ
0.0344 mole of NaโCoโ = 0.0344 mole of COโ
:. โ of mole = volume/ molar volume = 0.0344 = volume of COโ/22400cmยณ
=771cmยณ
========================================
(2ai)
[TABULATE]
=TEST=
C + heat
=OBSERVATION=
Formation of yellow flame
=INFERENCE=
Naโบ present
(2aii)
=TEST=
C + distilled water + shake
=OBSERVATION=
It readily dissolve in water
=INFERENCE=
C is a soluble in water
(2aiii)
=TEST=
Solution C + litmus paper
=OBSERVATION=
It changes moist red litmus to blue and no effect blue
=INFERENCE=
Solution C is alkaline
(2bi)
=TEST=
1st portion of solution C + barium chloride
=OBSERVATION=
White precipitate formed
=INFERENCE=
COโยฒโป , SOโยฒโป , Sยฒโป or SOโยฒโป
(2bii)
=TEST=
Add dilute HCl to product in (bi)
=OBSERVATION=
White precipitate dissolved
=INFERENCE=
COโ , SOโยฒโป or Sโยฒโป
(2biii)
=TEST=
To the second portion add phenolphthalein
=OBSERVATION=
Purple colour observed
=INFERENCE=
C is alkaline
========================================
(3ai)
Sulphur (iv) oxide and hydrogen sulphide.
(3aii)
Liberation of hydrogen gas with pop sound and formation of green iron (ii) chloride solution
(3aiii)
Spatula, beaker, weighing balance, standard volumetric flask
(3bi)
Solution turns red
(3bii)
Turns from brown to green
(3biii)
A colourless, odourless, acidic gas liberated which turns blue litmus paper red and turn lime water milky.
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